ISO 9504:1993

Metallurgical-grade fluorspar — Determination of antimony content — Solvent extraction atomic absorption spectrometric method

Publication date:   Apr 1, 1993

95.99   Withdrawal of Standard   Mar 3, 2010

General information

95.99   Withdrawal of Standard   Mar 3, 2010

ISO

ISO/TC 175 Fluorspar

International Standard

73.080   Non-metalliferous minerals

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Scope

The principle of the method specified is to decompose a test portion by a mixture of nitric, hydrofluoric and perchloric acids, dissolving the salts in hydrochloric acid after evaporation to fumes of sulfuric acid, extracting the antimony from a dilute hydrochloric acid solution of the decomposed test portion into a solution of tri-n-octylphosphine oxide in 4-methyl-2-pentanone, aspirating the extract into the air/acetylene flame of an atomic absorption spectrometer, and measuring the absorbance at 217,6 nm. Applies to products having an antimony content equal to or greater than 0,001 % (m/m).

Life cycle

PREVIOUSLY

WITHDRAWN
ISO 9504:1990

NOW

WITHDRAWN
ISO 9504:1993
95.99 Withdrawal of Standard
Mar 3, 2010