ISO 9061:1993

Acid-grade and ceramic-grade fluorspar — Determination of iron content — 1,10-Phenanthroline spectrometric method

Publication date:   Mar 18, 1993

95.99   Withdrawal of Standard   Mar 3, 2010

General information

95.99   Withdrawal of Standard   Mar 3, 2010

ISO

ISO/TC 175 Fluorspar

International Standard

73.080   Non-metalliferous minerals

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Scope

The method specified is based on alkaline fusion of a test portion with a mixture of sodium carbonate and boric acid, dissolution of the melt in excess hydrochloric acid, reduction of the iron(III) with hydroxylammonium chloride, formation of the iron(II)-1,10-phenanthroline complex in a buffered medium (pH between 3 and 5), spectrometric measurement of the absorbance of the coloured complex at a wavelength of about 510 nm, corresponding to the absorption maximum. Applies to products having iron contents, expressed as Fe2O3, in the range 0,1 % (m/m) to 2,0 % (m/m).

Life cycle

PREVIOUSLY

WITHDRAWN
ISO 9061:1988

NOW

WITHDRAWN
ISO 9061:1993
95.99 Withdrawal of Standard
Mar 3, 2010